Inorganica Chimica Acta
Inorganica Chimica Acta
3 years ago

Novel ligands, benzophenone N(4)-methyl-N(4)-phenylthiosemicarbazone, 1-(amino-N-methylphenylmethanethio)(diphenylmethylene)thiocarbonohydrazide and the transition metal complexes of the latter

Novel ligands, benzophenone N(4)-methyl-N(4)-phenylthiosemicarbazone, 1-(amino-N-methylphenylmethanethio)(diphenylmethylene)thiocarbonohydrazide and the transition metal complexes of the latter
Two Schiff base ligands, benzophenone N(4)-methyl-N(4)-phenylthiosemicarbazone (HL), 1-(amino-N-methyl-N-phenylmethanethio)(diphenylmethylene)thiocarbonohydrazide (H2L′) were synthesized. They were characterized by elemental analyses and spectral [Electronic, FT-IR, FT-Raman and 1H NMR] studies. The structure of HL was determined by single-crystal X-ray diffraction studies. The complexes of Co(II), Ni(II), Cu(II) and Zn(II) of H2L′ were synthesized. They were characterized by the elemental analyses, magnetic susceptibility, IR, electronic, NMR and thermal (TGA) studies. The crystal structure of Ni(HL′)2·1.5H2O was determined by single-crystal X-ray diffraction.

Publisher URL: www.sciencedirect.com/science

DOI: S0020169317308204

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