5 years ago

High-Pressure Synthesis of the First Ternary Melilite-Type Compound Sc1.67B3O7

High-Pressure Synthesis of the First Ternary Melilite-Type Compound Sc1.67B3O7
Kevin Ploner, Clivia Hejny, Martin K. Schmitt, Hubert Huppertz
Sc1.67B3O7 was synthesized in a high-pressure/high-temperature experiment at 3.5 GPa/1200 °C employing a Walker-type multianvil module. The compound was characterized with X-ray diffraction and vibrational spectroscopy. It crystallizes in the tetragonal, acentric space group P421m (no. 113) with the lattice parameters a = 6.6597(4) and c = 4.4364(3) Å. Sc1.67B3O7 is the first ternary compound adopting the melilite-type structure and therefore the simplest representative of this manifold structure family.

Publisher URL: http://onlinelibrary.wiley.com/resolve/doi

DOI: 10.1002/zaac.201700184

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