4 years ago

H2SO4-Mediated Stereocontrolled Annulation of Oxygenated Naphthalenes and 4-Alkenols: One-Pot Synthesis of Tetanthrenes

H2SO4-Mediated Stereocontrolled Annulation of Oxygenated Naphthalenes and 4-Alkenols: One-Pot Synthesis of Tetanthrenes
Yu-Ting Hsiao, Meng-Yang Chang
H2SO4-mediated one-pot stereocontrolled (4 + 2) annulation of 4-alkenols and oxygenated naphthalenes provided tetanthrenes in CH2Cl2 at 25 °C for 10 h. The use of various Brønsted acids or Lewis acids was investigated for a facile and efficient transformation. A plausible mechanism has been proposed.

Publisher URL: http://dx.doi.org/10.1021/acs.joc.7b02291

DOI: 10.1021/acs.joc.7b02291

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