3 years ago

Regioselective protection of xylose for efficient synthesis of arabino-α-1,3-xylosides

Regioselective protection of xylose for efficient synthesis of arabino-α-1,3-xylosides
We reported here an efficient regioselective protection strategy for xylose with two-step successive protections on 4- and 2-OH. This method enables the expeditious preparation of various xylose building blocks (3a c, 5, 6). The rapid selective 2,4-protection especially facilitates the synthesis of 3-substituted xyloside structures. By this approach, typical arabino-α-1,3-xyloside disaccharide and trisaccharide, as fragment structure units from arabinoxylans, have been successfully synthesized.

Publisher URL: www.sciencedirect.com/science

DOI: S0040403917312479

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