5 years ago

Microwave-assisted synthesis of Ni, Zn layered double hydroxysalts

Microwave-assisted synthesis of Ni, Zn layered double hydroxysalts
Layered double hydroxysalts containing Ni2+ and Zn2+ cations and acetate as counterbalancing anions have been synthetised uner microwave irradiation. The samples have been analysed by element chemical analysis, powder X-ray diffraction, FT-IR and Vis-UV spectroscopies, determination of the specific surface area, and thermal analyses. The microwave procedure produces better crystallised materials and faster than by conventional hydrothermal treatment, although when the reaction time under microwave irradiation is prolonged a partial decomposition of the particles is observed.

Publisher URL: www.sciencedirect.com/science

DOI: S138718111730464X

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