5 years ago

New Approach to 1,4-Benzoxazin-3-ones by Electrochemical C−H Amination

New Approach to 1,4-Benzoxazin-3-ones by Electrochemical C−H Amination
Jun-ichi Yoshida, Sebastian Herold, Siegfried R. Waldvogel, Lars Julian Wesenberg, Akihiro Shimizu
Simple electrified access to benzoxazinones starting from readily accessible methyl phenoxyacetetes was established. Similar benzoxazine compounds occur naturally in gramineous plants such as wheat, maize, rye, or rice. The electrochemical amination protocol furnishes, upon aminolysis, the heterocyclic benzoxazinone motif. The simple electric wires underline the easy-to-perform protocol. More information can be found in the Communication by S. R. Waldvogel et al. (DOI: 10.1002/chem.201701979).

Publisher URL: http://onlinelibrary.wiley.com/resolve/doi

DOI: 10.1002/chem.201703421

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