Organic Letters
Organic Letters
5 years ago

Palladium-Catalyzed C(sp2)–H Acetoxylation via Electrochemical Oxidation

Palladium-Catalyzed C(sp2)–H Acetoxylation via Electrochemical Oxidation
Qi-Liang Yang, Dayong Zhang, Ping Fang, Tian-Sheng Mei, Yi-Qian Li
Palladium-catalyzed arene C(sp2)–H acetoxylation has emerged as a powerful tool to construct a carbon–oxygen (C–O) bond. However, the requirement of stoichiometric chemical oxidants for this transformation possesses a significant disadvantage. To solve this fundamental problem, we now report an anodic oxidation strategy to achieve arene C(sp2)–H acetoxylation.

Publisher URL: http://dx.doi.org/10.1021/acs.orglett.7b01138

DOI: 10.1021/acs.orglett.7b01138

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