3 years ago
Copper-Catalyzed TBHP-Mediated Radical Cross-Coupling Reaction of Sulfonylhydrazides with Thiols Leading to Thiosulfonates

Jian-Ping Zou, Shuai-Shuai Lv, Adedamola Shoberu, Guo-Yu Zhang
A tert-butyl hydroperoxide (TBHP)-mediated coupling of sulfonylhydrazides with thiols catalyzed by CuBr2 to afford thiosulfonates via a radical process is described.
Publisher URL: http://dx.doi.org/10.1021/acs.joc.7b01121
DOI: 10.1021/acs.joc.7b01121
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