Organic Letters
Organic Letters
5 years ago

One-Pot Method for the Synthesis of 2,5-Unsubstituted Pyrrolidino[3′,4′:1,9]fullerenes

One-Pot Method for the Synthesis of 2,5-Unsubstituted Pyrrolidino[3′,4′:1,9]fullerenes
Usein M. Dzhemilev, Airat R. Tuktarov, Zulfiya R. Shakirova
A new, efficient process has been developed for the preparation of 2,5-unsubstituted pyrrolidino[3′,4′:1,9]fullerenes by the Ti(O-i-Pr)4-promoted reaction of fullerene C60 with 1,3,5-perhydrotriazines generated in situ upon the reaction of primary alkyl- and benzylamines with paraformaldehyde and EtMgBr.

Publisher URL: http://dx.doi.org/10.1021/acs.orglett.7b01730

DOI: 10.1021/acs.orglett.7b01730

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